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Optical and electron microscopy has been used to characterise the ex-service material, with Energy Dispersive Analysis of X-rays (EDAX), image analysis and Electron Back Scattered Diffraction used to quantify the carbide phases through the tube wall, which can be correlated with the magnetic response and tube swelling.
Finite Element modelling of the carbon diffusion and carbide precipitation using phase equilibria predicted by Thermocalc for HP Nb alloy, is being used to incorporate damage accumulation rates caused by the carburisation into the global FEA models.